δ, ppm
|
Coupling constant Hz
|
ppm
|
1
|
|
|
N.D.
|
2
|
2.347
|
m
|
34.298
|
3
|
2.39
|
m
|
23.022
|
4
|
5.406
|
m
|
128.300
|
5
|
5.409
|
m
|
129.047
|
6
|
2.822
|
t, J(6,5)=J(6,7)=5.35
|
25.704
|
7
|
5.467
|
m
|
130.009
|
8
|
5.461
|
m
|
125.516
|
9
|
2.4
|
m, J(9,10)=6.5
|
35.350
|
10
|
4.198
|
J(10,11)=6.3, J(10,12)=1.3
|
72.043
|
11
|
5.757
|
J(11,12)=15
|
137.127
|
12
|
6.747
|
J(12,13)=11, J(12,14)=-0.8
|
125.476
|
13
|
5.991
|
J(13,14)=11, J(13,15)=-0.8
|
128.966
|
14
|
5.995
|
J(14,15)=11
|
128.985
|
15
|
6.741
|
J(15,16)=15, J(15,17) =1.3
|
125.476
|
16
|
5.744
|
J(16,17)=6.3
|
137.066
|
17
|
4.174
|
J(17,18)=6.5
|
72.142
|
18
|
2.320
|
m
|
35.210
|
19
|
5.387
|
m
|
124.446
|
20
|
5.493
|
m
|
133.674
|
21
|
1.2
|
J(21,22)=7.05
|
20.667
|
22
|
0.983
|
7.5
|
13.518
|
Figure 1
Figure 2
Figure 3:
Figure 4:
Figure 5:
Figure 7:
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