Title:Effect of epoxy resin on the thermal behaviors and viscoelastic properties of poly(phenylene sulfide)
Authors:Wu, Defeng (1); Wu, Lanfeng (1); Wang, Jianghong (1); Sun, Yurong (1); Zhang, Ming (1)
Author affiliation:(1) School of Chemistry and Chemical Engineering, Shouxihu Campus, Yangzhou University, Yangzhou, Jiangsu 225002, China
Publisher:Elsevier Ltd, Langford Lane, Kidlington, Oxford, OX5 1GB, United Kingdom
Abstract:In this work, thermal behaviors and viscoelasticity of the PPS/epoxy resin mixtures prepared by melt mixing were studied, and the rheology was used as a tool to further explore the relation between chain structures and properties of the mixtures. The results show that the epoxy resin can promotes degradation and branching of the PPS during melt mixing due to its poor thermal stability. The formation of long chain branched and partly crosslinked structures in the mixtures together with the residual decomposed components hence result in broadening of molecular weight distribution in comparison with those of the neat PPS. As a consequence, the mixtures show the viscoelastic behaviors far different from the neat PPS: the presence of crosslinked structure leads to the strong solid-like responses in the small amplitude oscillatory shear (SAOS) flow, and the presence of long chain branched structure to the weak strain overshoots in the large amplitude oscillatory shear (LAOS) flow. Moreover, after quiescent annealing, a strain-scaling transient stress behavior is observed in the mixtures in the reverse flow. © 2011 Published by Elsevier B.V.
Controlled terms:Aromatic compounds - Elasticity - Epoxy resins - Mixtures - Molecular mass - Molecular weight distribution - Polyethylenes - Polymer blends - Shear stress - Synthetic resins - Viscoelasticity - Viscosity
Uncontrolled terms:Chain structure - Crosslinked structures - Large amplitude oscillatory shear - Long chain branched structures - Long chains - Melt mixing - Oscillatory shear - Poly(phenylene sulfide) - Quiescent annealing - Resin mixtures - Reverse flow - Small amplitude - Thermal behaviors - Thermal stability - Transient stress - Viscoelastic behaviors - Viscoelastic properties
Classification code:815.1.1 Organic Polymers - 815.1 Polymeric Materials - 804.1 Organic Compounds - 802.3 Chemical Operations - 801 Chemistry - 631.1 Fluid Flow, General - 421 Strength of Building Materials; Mechanical Properties
Compilation and indexing terms, Copyright 2011 Elsevier Inc.
Authors:Yang, Zhanjun (1); Ren, Yanyan (1); Zhang, Yongcai (1); Li, Juan (1); Li, Hongbo (1); Hu, Xiaochun Huang Xiaoya (1); Xu, Qin (1)
Author affiliation:(1) College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China
Abbreviated source title:Biosens. Bioelectron.
Publisher:Elsevier Ltd, Langford Lane, Kidlington, Oxford, OX5 1GB, United Kingdom
Abstract:A novel biosensor is developed based on immobilization of proteins on nanoflake-like SnS2 modified glass carbon electrode (GCE). With glucose oxidase (GOD) as a model, direct electrochemistry of the GOD/nanoflake-like SnS2 is studied. The prepared SnS2 has large surface area and can offer favorable microenvironment for facilitating the electron transfer between protein and electrode surface. The properties of GOD/SnS2 are characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), UV-vis spectroscopy, Fourier transform infrared spectroscopy (FTIR) and cyclic voltammetry (CV), respectively. The immobilized enzyme on nanoflake-like SnS2 retains its native structure and bioactivity and exhibits a surface-controlled, reversible two-proton and two-electron transfer reaction with the apparent electron transfer rate constant (ks) of 3.68s-1. The proposed biosensor shows fast amperometric response (8s) to glucose with a wide linear range from 2.5×10-5M to 1.1×10-3M, a low detection limit of 1.0×10-5M at signal-to-noise of 3 and good sensitivity (7.6±0.5mAM-1cm-2). The resulting biosensor has acceptable operational stability, good reproducibility and excellent selectivity and can be successfully applied in the reagentless glucose sensing at -0.45V. It should be worthwhile noting that it opens a new avenue for fabricating excellent electrochemical biosensor. © 2011 Elsevier B.V.
Controlled terms:Cyclic voltammetry - Electrochemistry - Electrodes - Electrolysis - Electron transitions - Fourier transform infrared spectroscopy - Glucose - Glucose sensors - Rate constants - Scanning electron microscopy - Ultraviolet spectroscopy - X ray diffraction
Uncontrolled terms:Amperometric response - Biosensing - Direct electrochemistry - Electrochemical biosensor - Electrode surfaces - Electron transfer - Electron-transfer rate constants - FTIR - Glass carbon electrodes - Glucose sensing - Immobilized enzyme - Large surface area - Low detection limit - matrix - Microenvironments - Nanoflake-like SnS2 - Native structures - Operational stability - Reagent-less - Reproducibilities - Signal to noise - Two-electron transfer - UV-vis spectroscopy - Wide-linear range
Classification code:931.3 Atomic and Molecular Physics - 804.1 Organic Compounds - 801 Chemistry - 741.1 Light/Optics - 711.1 Electromagnetic Waves in Different Media - 704.1 Electric Components - 461.9 Biology
Compilation and indexing terms, Copyright 2011 Elsevier Inc.
Accession number:20112714122418
Title:Optimization design of construction machinery based on ansys
Authors:Wang, Guoqing (1); Chen, Jingxin (1)
Author affiliation:(1) College of Mechanical Engineering, Yangzhou University, Yangzhou 225127, Jiangsu, China
Corresponding author:Wang, G.(carl_won@163.com)
Source title:2011 International Conference on Electric Information and Control Engineering, ICEICE 2011 - Proceedings
Abbreviated source title:Int. Conf. Electr. Inf. Control Eng., ICEICE - Proc.
Monograph title:2011 International Conference on Electric Information and Control Engineering, ICEICE 2011 - Proceedings
Issue date:2011
Publication year:2011
Pages:5166-5169
Article number:5777015
Language:Chinese
ISBN-13:9781424480395
Document type:Conference article (CA)
Conference name:2011 International Conference on Electric Information and Control Engineering, ICEICE 2011
Conference date:April 15, 2011 - April 17, 2011
Conference location:Wuhan, China
Conference code:85257
Sponsor:IEEE Beijing Section ED Chapter; Jiangsu University
Publisher:IEEE Computer Society, 445 Hoes Lane - P.O.Box 1331, Piscataway, NJ 08855-1331, United States
Abstract:Through the introduction of continuous variable density topology optimization, try to use it in product development and optimization of large-scale mechanical product, and put forward the optimization theory, method and practical experience. © 2011 IEEE.
Number of references:10
Main heading:Optimization
Controlled terms:Computer aided engineering - Construction equipment - Machine design - Machinery - Product development - Site selection - Topology
Uncontrolled terms:ansys - construction Machinery - Continuous variables - Mechanical product - Optimization design - Optimization theory - Practical experience
Classification code:921.4 Combinatorial Mathematics, Includes Graph Theory, Set Theory - 913.1 Production Engineering - 723.5 Computer Applications - 921.5 Optimization Techniques - 601 Mechanical Design - 403 Urban and Regional Planning and Development - 402 Buildings and Towers - 405.1 Construction Equipment
DOI:10.1109/ICEICE.2011.5777015
Database:Compendex
Compilation and indexing terms, Copyright 2011 Elsevier Inc.
Accession number:20112714122000
Title:Dynamic hand gesture recognition based on SURF tracking
Authors:Bao, Jiatong (1); Song, Aiguo (1); Guo, Yan (1); Tang, Hongru (2)
Author affiliation:(1) School of Instrument Science and Engineering, Southeast University, Nanjing, Jiangsu Province, China; (2) School of Energy and Power Engineering, Yangzhou University, Yangzhou, Jiangsu Province, China
Corresponding author:Bao, J.(seu.bjt@163.com)
Source title:2011 International Conference on Electric Information and Control Engineering, ICEICE 2011 - Proceedings
Abbreviated source title:Int. Conf. Electr. Inf. Control Eng., ICEICE - Proc.
Monograph title:2011 International Conference on Electric Information and Control Engineering, ICEICE 2011 - Proceedings
Issue date:2011
Publication year:2011
Pages:338-341
Article number:5777598
Language:English
ISBN-13:9781424480395
Document type:Conference article (CA)
Conference name:2011 International Conference on Electric Information and Control Engineering, ICEICE 2011
Conference date:April 15, 2011 - April 17, 2011
Conference location:Wuhan, China
Conference code:85257
Sponsor:IEEE Beijing Section ED Chapter; Jiangsu University
Publisher:IEEE Computer Society, 445 Hoes Lane - P.O.Box 1331, Piscataway, NJ 08855-1331, United States
Abstract:A novel method of dynamic hand gesture recognition based on Speeded Up Robust Features (SURF) tracking is proposed. The main characteristic is that the dominant movement direction of matched SURF points in adjacent frames is used to help describing a hand trajectory without detecting and segmenting the hand region. The dynamic hand gesture is then modeled by a series of trajectory direction data streams after time warping. Accordingly, the data stream clustering method based on correlation analysis is developed to recognize a dynamic hand gesture and to speed up calculation. The proposed algorithm is tested on 26 alphabetical hand gestures and yields a satisfactory recognition rate which is 87.1% on the training set and 84.6% on the testing set. © 2011 IEEE.
Number of references:13
Main heading:Gesture recognition
Controlled terms:Algorithms - Data communication systems - Feature extraction
Uncontrolled terms:Correlation analysis - Data stream - Data stream clustering - Feature-tracking - Hand gesture - Hand-gesture recognition - Main characteristics - Novel methods - Recognition rates - Speed-ups - Speeded up robust features - SURF - Time warping - Training sets
Classification code:716 Telecommunication; Radar, Radio and Television - 717 Optical Communication - 718 Telephone Systems and Related Technologies; Line Communications - 723 Computer Software, Data Handling and Applications - 921 Mathematics
DOI:10.1109/ICEICE.2011.5777598
Database:Compendex
Compilation and indexing terms, Copyright 2011 Elsevier Inc.
Accession number:20112714113877
Title:Performance of the nail joints on wood frame shear walls
Authors:Liu, Yan (1); Zou, Xiaojin (1); She, Chengang (1)
Author affiliation:(1) School of Civil Engineering, Yangzhou University, Yangzhou, Jiangsu Province 225009, China; (2) College of Wood Science and Technology, Nanjing Forestry University, Nanjing 210037, China; (3) College of Civil Engineering, Nanjing University of Technology, Nanjing 210009, China
Corresponding author:Liu, Y.(liuyan@yzu.edu.cn)
Source title:Advanced Materials Research
Abbreviated source title:Adv. Mater. Res.
Volume:255-260
Monograph title:Advances in Civil Engineering
Issue date:2011
Publication year:2011
Pages:350-354
Language:English
ISSN:10226680
ISBN-13:9783037851395
Document type:Conference article (CA)
Conference name:2011 International Conference on Civil Engineering and Building Materials, CEBM 2011
Conference date:July 29, 2011 - July 31, 2011
Conference location:Kunming, China
Conference code:85320
Sponsor:Kunming University of Science and Technology; International Association for Scientific and High Technology
Publisher:Trans Tech Publications, P.O. Box 1254, Clausthal-Zellerfeld, D-38670, Germany
Abstract:The performance of two types of Chinese screw nails in connections between sheathing and wood frame was assessed using ASTM-F1575-03. Specimens were tested in groups of 10, and both parallel-to-grain and perpendicular-to-grain specimens were tested in the case of ASTMF1676-03. It was found that the type of nail had little effect on the performance of nail joints. Finally a modified model suitable to domestic nails in two directions was established on the basis of Foschi's exponential model. The model provides useful data on the performance of sheathing-tolumber connections. © (2011) Trans Tech Publications, Switzerland.
Number of references:6
Main heading:Building materials
Controlled terms:Civil engineering - Construction equipment - Earthquake effects
Uncontrolled terms:Exponential models - Mode - Modified model - Test research - Two directions - Wood frame
Classification code:415 Metals, Plastics, Wood and Other Structural Materials - 414 Masonry Materials - 413 Insulating Materials - 484 Seismology - 412 Concrete - 409 Civil Engineering, General - 405.1 Construction Equipment - 411 Bituminous Materials
DOI:10.4028/www.scientific.net/AMR.255-260.350
Database:Compendex
Compilation and indexing terms, Copyright 2011 Elsevier Inc.
Accession number:20113214224589
Title:Experimental research on cold extruding of internal thread in Q460 high-strength-steel
Authors:Miao, Hong (1); Zuo, Dunwen (2); Zhang, Ruihong (1); Wang, Min (2)
Author affiliation:(1) College of Mechanical Engineering, Yangzhou University, Yangzhou 225000, China; (2) College of Mechanical and Electrical Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Corresponding author:Miao, H.(mh0514@163.com)
Source title:Jixie Gongcheng Xuebao/Journal of Mechanical Engineering
Abbreviated source title:Jixie Gongcheng Xuebao
Volume:47
Issue:13
Issue date:July 5, 2011
Publication year:2011
Pages:160-166
Language:Chinese
ISSN:05776686
CODEN:CHHKA2
Document type:Journal article (JA)
Publisher:Editorial Office of Chinese Journal of Mechanical, 22 Baiwanzhuang Dajie, Beijing, 100037, China
Abstract:Traditional cold extrusion process of internal thread is only fit for processing low-intensity and high plasticity metals such as non-ferrous metals and low-carbon steel. But the internal thread of the key parts such as airplane and high speed train is processed with high-strength steel. During cold extruding high-strength steel internal thread, the effects of lubricant, workpiece bottom hole diameter, extrusion speed and extrusion times on wear and fracture of the tap and manufacturing quality of the internal thread are great. The process of cold extrusion of Q460 high-strength steel internal thread is studied through experiments. The effects of lubricant, workpiece bottom hole diameter, extrusion speed and extrusion times on extrusion torque and extrusion temperature is analyzed. And the ideal internal thread is obtained through optimizing technological parameters. It provides a new basis for improving the surface quality and the fatigue property of internal thread. The test results show that Q460 high-strength steel internal thread is better formed by cold extrusion through one-step forming technology. The fluidic thin film lubricant whose viscosity number is between 10 and 12 is selected. The best range of workpiece bottom hole diameter is between 21.20 mm and 21.30 mm. And the generally selected extrusion speed is between 30 and 60 mm · min-1. ©2011 Journal of Mechanical Engineering.
Number of references:10
Main heading:High strength steel
Controlled terms:Extrusion - Low carbon steel
Uncontrolled terms:Bottom hole - Cold extrusion - Cold extrusion process - Experimental research - Extrusion speed - Extrusion temperatures - Fatigue properties - Forming technology - High plasticity - High speed trains - Internal threads - Key parts - Low-intensity - Manufacturing quality - Technological parameters - Test results - Work pieces
Classification code:535.2.2 Metal Forming Practice - 545.3 Steel
DOI:10.3901/JME.2011.13.160
Database:Compendex
Compilation and indexing terms, Copyright 2011 Elsevier Inc.
Accession number:20112714113564
Title:Elimination of chromatic aberration and tuning of the saturation in reflective flat-panel display by utilizing monodisperse colloidal crystal beads as pixels
Authors:Sun, Cheng (1); Yao, Yunhong (1); Sun, Liguo (2); Gu, Zhongze (2)
Author affiliation:(1) College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China; (2) State Key Laboratory of Bioelectronics, Southeast University, Nanjing 210096, China
Corresponding author:Sun, C.(suncheng@yzu.edu.cn)
Source title:Colloids and Surfaces A: Physicochemical and Engineering Aspects
Abbreviated source title:Colloids Surf. A Physicochem. Eng. Asp.
Volume:384
Issue:1-3
Issue date:July 5, 2011
Publication year:2011
Pages:720-725
Language:English
ISSN:09277757
E-ISSN:18734359
CODEN:CPEAEH
Document type:Journal article (JA)
Publisher:Elsevier, P.O. Box 211, Amsterdam, 1000 AE, Netherlands
Abstract:We proposed an idea for overcoming the difficulties met by the application of colloidal photonic crystal in flat-panel displays, such as overcoming the viewing angle dependence, displaying a complicated image, and, how to control the brightness and saturation of each pixel. In our strategy, nanospheres were firstly self-assembled into uniform spherical units, and then the colloidal crystal units were patterned as pixels. This method was favorable to realize the fabrication of display device in a large scale, with controllable uniformity and easily pattern designing. The problem that display colors varies with the observation angle can probably be adequately corrected through the homogeneity derived from the spherical symmetry of the colloidal crystals. Nematic liquid crystals were infiltrated into the voids of the inverse opaline colloidal crystal unit, and the saturation of the pixels can be controlled by utilizing the field response feature of the liquid crystals. © 2011 Elsevier B.V.